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Resin Behaviour During Processing: What are the key resin properties to consider when developing a manufacturing process? - A257

From CKN Knowledge in Practice Centre
Perspectives - A8AIM Events - Webinars - A115Resin Behaviour During Processing: What are the key resin properties to consider when developing a manufacturing process? - A257
 
Resin Behaviour During Processing: What are the key resin properties to consider when developing a manufacturing process?
Perspectives article
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Document Type Article
Document Identifier 257
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Prerequisites
Webinar Date
  • June 16, 2021

Introduction[edit | edit source]

During manufacturing the resin undergoes significant transformations: thermoset resins evolve from a low molecular weight liquid to a highly cross-linked solid. A thorough understanding of this liquid-to-solid transition is critical when developing, optimizing or troubleshooting a manufacturing process. For example, the impregnation and consolidation of the fiber bed must be completed before the resin transforms from a viscous liquid to a rubbery gel, and demolding must happen when the resin reaches a glassy solid state.

This webinar discusses the key manufacturing properties of thermoset resins such as viscosity, gelation, glass transition temperature, and degree of cure. Short videos are used to demonstrate the different techniques used today to characterize these manufacturing properties. The content of this webinar will be extracted live from the Knowledge in Practice Centre (KPC) – an open resource for composites manufacturing knowledge and best practices, available online at https://compositeskn.org/KPC.

Webinar[edit | edit source]

Webinar slides[edit | edit source]

Webinar slides available by clicking on the icon below

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Additional information for select chapters[edit | edit source]

Chapter Chapter Title Links to related information in the Knowledge in Practice Centre
1 Welcome & introductions N/A
2 Overview of the Knowledge in Practice Centre (KPC)
3 Outline and learning objectives N/A
4 How does the resin transform during manufacturing
5 What are the key resin properties to consider? N/A
6 Example manufacturing workflow (RTM)
7 Impregnation step Future content
8 Viscosity
9 Gel time
10 Thermal transformation (curing) step
11 Degree of cure
12 Heat of reaction
13 Demoulding step Future content
14 Glass transition temperature
15 Assembly step Future content
16 Thermo-volumetric behaviour
17 Commonly available information from data sheets N/A
18 Example TDS: Vinyl ester resin Future content
19 Example TDS: Epoxy prepreg Future content
20 Characterizing material properties: Gel time
21 Characterizing material properties: Degree of cure
22 Characterizing material properties: Viscosity
23 Summary & wrap-up N/A
24 Q&A N/A


Related pages

Page type Links
Introduction to Composites Articles
Foundational Knowledge Articles
Foundational Knowledge Method Documents
Foundational Knowledge Worked Examples
Systems Knowledge Articles
Systems Knowledge Method Documents
Systems Knowledge Worked Examples
Systems Catalogue Articles
Systems Catalogue Objects – Material
Systems Catalogue Objects – Shape
Systems Catalogue Objects – Tooling and consumables
Systems Catalogue Objects – Equipment
Practice Documents
Case Studies
Perspectives Articles


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Welcome

Welcome to the CKN Knowledge in Practice Centre (KPC). The KPC is a resource for learning and applying scientific knowledge to the practice of composites manufacturing. As you navigate around the KPC, refer back to the information on this right-hand pane as a resource for understanding the intricacies of composites processing and why the KPC is laid out in the way that it is. The following video explains the KPC approach:

Understanding Composites Processing

The Knowledge in Practice Centre (KPC) is centered around a structured method of thinking about composite material manufacturing. From the top down, the heirarchy consists of:

The way that the material, shape, tooling & consumables and equipment (abbreviated as MSTE) interact with each other during a process step is critical to the outcome of the manufacturing step, and ultimately critical to the quality of the finished part. The interactions between MSTE during a process step can be numerous and complex, but the Knowledge in Practice Centre aims to make you aware of these interactions, understand how one parameter affects another, and understand how to analyze the problem using a systems based approach. Using this approach, the factory can then be developed with a complete understanding and control of all interactions.

The relationship between material, shape, tooling & consumables and equipment during a process step


Interrelationship of Function, Shape, Material & Process

Design for manufacturing is critical to ensuring the producibility of a part. Trouble arises when it is considered too late or not at all in the design process. Conversely, process design (controlling the interactions between shape, material, tooling & consumables and equipment to achieve a desired outcome) must always consider the shape and material of the part. Ashby has developed and popularized the approach linking design (function) to the choice of material and shape, which influence the process selected and vice versa, as shown below:

The relationship between function, material, shape and process


Within the Knowledge in Practice Centre the same methodology is applied but the process is more fully defined by also explicitly calling out the equipment and tooling & consumables. Note that in common usage, a process which consists of many steps can be arbitrarily defined by just one step, e.g. "spray-up". Though convenient, this can be misleading.

The relationship between function, material, shape and process consisting of Equipment and Tooling and consumables


Workflows

The KPC's Practice and Case Study volumes consist of three types of workflows:

  • Development - Analyzing the interactions between MSTE in the process steps to make decisions on processing parameters and understanding how the process steps and factory cells fit within the factory.
  • Troubleshooting - Guiding you to possible causes of processing issues affecting either cost, rate or quality and directing you to the most appropriate development workflow to improve the process
  • Optimization - An expansion on the development workflows where a larger number of options are considered to achieve the best mixture of cost, rate & quality for your application.